Modernizing Ignitable Liquids Determinations

Published date02 April 2019
Citation84 FR 12539
Record Number2019-05878
SectionProposed rules
CourtEnvironmental Protection Agency
12539
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
consistent with the fundamental
federalism principles and preemption
requirements described in Executive
Order 13132.
Also, this proposed rule does not have
tribal implications under Executive
Order 13175, Consultation and
Coordination with Indian Tribal
Governments, because it would not have
a substantial direct effect on one or
more Indian tribes, on the relationship
between the Federal Government and
Indian tribes, or on the distribution of
power and responsibilities between the
Federal Government and Indian tribes.
If you believe this proposed rule has
implications for federalism or Indian
tribes, please contact the person listed
in the
FOR FURTHER INFORMATION
CONTACT
section.
E. Unfunded Mandates Reform Act
The Unfunded Mandates Reform Act
of 1995 (2 U.S.C. 1531–1538) requires
Federal agencies to assess the effects of
their discretionary regulatory actions. In
particular, the Act addresses actions
that may result in the expenditure by a
State, local, or tribal government, in the
aggregate, or by the private sector of
$100,000,000 (adjusted for inflation) or
more in any one year. Though this
proposed rule would not result in such
an expenditure, we do discuss the
effects of this rule elsewhere in this
preamble.
F. Environment
We have analyzed this proposed rule
under Department of Homeland
Security Directive 023–01 and
Commandant Instruction M16475.1D,
which guide the Coast Guard in
complying with the National
Environmental Policy Act of 1969 (42
U.S.C. 4321–4370f), and have made a
preliminary determination that this
action is one of a category of actions that
do not individually or cumulatively
have a significant effect on the human
environment. This proposed rule
involves a safety zone that allows all
vessels to transit or navigate within the
safety zone but prohibits vessels, other
than large passenger vessels from
anchoring within the safety zone
without the express consent from the
Captain of the Port, Southeast Alaska or
a designated representative. Normally
such actions are categorically excluded
from further review under paragraph
L60(a) of Appendix A, Table 1 of DHS
Instruction Manual 023–01–001–01,
Rev. 01 We seek any comments or
information that may lead to the
discovery of a significant environmental
impact from this proposed rule.
V. Public Participation and Request for
Comments
We view public participation as
essential to effective rulemaking, and
will consider all comments and material
received during the comment period.
Your comment can help shape the
outcome of this rulemaking. If you
submit a comment, please include the
docket number for this rulemaking,
indicate the specific section of this
document to which each comment
applies, and provide a reason for each
suggestion or recommendation.
We encourage you to submit
comments through the Federal
eRulemaking Portal at http://
www.regulations.gov. If your material
cannot be submitted using http://
www.regulations.gov, contact the person
in the
FOR FURTHER INFORMATION
CONTACT
section of this document for
alternate instructions.
We accept anonymous comments. All
comments received will be posted
without change to https://
www.regulations.gov and will include
any personal information you have
provided. For more about privacy and
the docket, visit https://
www.regulations.gov/privacyNotice.
Documents mentioned in this NPRM
as being available in the docket, and all
public comments, will be in our online
docket at https://www.regulations.gov
and can be viewed by following that
website’s instructions. Additionally, if
you go to the online docket and sign up
for email alerts, you will be notified
when comments are posted or a final
rule is published.
List of Subjects in 33 CFR Part 165
Harbors, Marine safety, Navigation
(water), Reporting and recordkeeping
requirements, Security measures,
Waterways.
For the reasons discussed in the
preamble, the Coast Guard is proposing
to amend 33 CFR part 165 as follows:
PART 165—REGULATED NAVIGATION
AREAS AND LIMITED ACCESS
AREAS.
1. The authority citation for part 165
continues to read as follows:
Authority: 33 U.S.C. 1231; 50 U.S.C. 191;
33 CFR 1.05–1, 6.04–1, 6.04–6, and 160.5;
Department of Homeland Security Delegation
No. 0170.1.
2. Revise § 165.1702 to read as
follows:
§ 165.1702 Gastineau Channel, Juneau,
Alaska-safety zone.
(a) The waters within the following
boundaries are a safety zone: All waters
eastward to shore from a line beginning
at Gastineau Channel Light 4 (LLNR
23695) in position 58°17.82N,
134°25.36W, in the direction of 130°
True to Rock Dump Lighted Buoy 2A
(LLNR 23685) at position 58°17.14N,
134°23.84W.
(b) Definitions. The following
definitions apply to this section:
(1) A large passenger vessel for the
purpose of this regulation are cruise
ships and ferries.
(2) Cruise ship means any vessel over
100 gross registered tons, carrying more
than 12 passengers for hire which makes
voyages lasting 24 hours, of which any
part is on high seas. Passengers from
cruise ships are embarked or
disembarked in the U.S. or its
territories. Cruise ships do not include
ferries that hold Coast Guard Certificates
of Inspection endorsed for ‘‘Lakes, Bays,
And Sounds’’, that transit international
waters for only short periods of time on
frequent schedules.
(3) Ferry means a vessel which is
limited in its use to the carriage of deck
passengers or vehicles or both, operates
on a short run on a frequent schedule
between two or more points over the
most direct water route, other than in
ocean or coastwise service.
(c) Special Regulations. (1) All vessels
may transit or navigate within the safety
zone.
(2) No vessels, other than a large
passenger vessel may anchor within the
safety zone without the express consent
from the Captain of the Port, Southeast
Alaska.
Dated: March 7, 2019.
Stephen R. White,
Capt., U.S. Coast Guard, Captain of the Port,
Southeast Alaska.
[FR Doc. 2019–06375 Filed 4–1–19; 8:45 am]
BILLING CODE 9110–04–P
ENVIRONMENTAL PROTECTION
AGENCY
40 CFR Parts 260, 261, and 266
[EPA–HQ–OLEM–2018–0830; FRL–9991–
43–OLEM]
RIN 2050–AG93
Modernizing Ignitable Liquids
Determinations
AGENCY
: Environmental Protection
Agency (EPA).
ACTION
: Proposed rule.
SUMMARY
: The Environmental Protection
Agency (EPA or the Agency) is
proposing to update the regulations for
the identification of ignitable hazardous
waste under the Resource Conservation
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00013 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12540
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
and Recovery Act (RCRA) and to
modernize the RCRA test methods that
currently require the use of mercury
thermometers. These proposed revisions
would provide greater clarity to
hazardous waste identification, provide
flexibility in testing requirements,
improve environmental compliance,
and, thereby, enhance protection of
human health and the environment.
DATES
: Comments must be received on
or before June 3, 2019.
ADDRESSES
: Submit your comments,
identified by Docket ID No. EPA–HQ–
OLEM–2018–0830, at http://
www.regulations.gov. Follow the online
instructions for submitting comments.
Once submitted, comments cannot be
edited or removed from Regulations.gov.
The EPA may publish any comment
received to its public docket. Do not
submit electronically any information
you consider to be Confidential
Business Information (CBI) or other
information whose disclosure is
restricted by statute. Multimedia
submissions (audio, video, etc.) must be
accompanied by a written comment.
The written comment is considered the
official comment and should include
discussion of all points you wish to
make. The EPA will generally not
consider comments or comment
contents located outside of the primary
submission (i.e., on the web, cloud, or
other file sharing system). For
additional submission methods, the full
EPA public comment policy,
information about CBI or multimedia
submissions, and general guidance on
making effective comments, please visit
https://www.epa.gov/dockets/
commenting-epa-dockets.
FOR FURTHER INFORMATION CONTACT
:
Daniel Fagnant, Office of Land and
Emergency Management (5304P),
Environmental Protection Agency, 1200
Pennsylvania Avenue NW, Washington,
DC 20460; telephone number 703–308–
0319; email address: fagnant.daniel@
epa.gov or Melissa Kaps, Office of Land
and Emergency Management (5304P),
Environmental Protection Agency, 1200
Pennsylvania Avenue NW, Washington,
DC 20460; telephone number 703–308–
6787; email address: kaps.melissa@
epa.gov.
SUPPLEMENTARY INFORMATION
: The
information presented in this preamble
is organized as follows:
I. General Information
A. Does this action apply to me?
B. What action is the Agency taking?
C. What is the Agency’s authority for
taking this action?
D. What are the incremental costs and
benefits of this action?
II. Background
A. What is a hazardous waste?
B. What is the hazardous waste
characteristic of ignitability?
C. What is the regulatory history of the
ignitability characteristic?
D. What is a flash point and how is it
measured?
E. What flash point test methods does EPA
currently require?
F. What is the aqueous alcohol exclusion?
G. Why consider alternatives to mercury
thermometers in test methods?
III. Proposed Revisions to the Ignitability
Characteristic Flash Point Test Methods
A. Why is EPA proposing new flash point
test methods for ignitable liquids?
B. What test method is EPA proposing to
add to Method 1010A?
C. What test method is EPA proposing to
add to Method 1020B?
D. How are the proposed test methods
equivalent to the currently required test
methods?
E. Why is EPA not removing the currently
required flash point test methods?
IV. Codification of Guidance Into the
Ignitability Characteristic
A. Aqueous Alcohol Exclusion
1. Why is EPA proposing a revision to the
aqueous alcohol exclusion?
2. What are the proposed changes to the
aqueous alcohol exclusion?
3. Solicitation of Public Input on Other
Changes to the Aqueous Alcohol
Exclusion for Ignitability
B. Multiphase Testing
1. Why is the Agency proposing a revision
to codify sampling guidance for
multiphase wastes?
2. Proposed Codification of Guidance for
Multiphase Waste Sampling
V. Additional Corrections to § 261.21
A. What are the proposed changes to the
definition of ignitable compressed gas in
§ 261.21(a)(3)(ii)?
B. What are the proposed changes to
§ 261.21(a)(4)(i)(A)?
C. What are the proposed changes to the
notes section of § 261.21?
VI. Revision to Mercury Thermometer
Requirements in the Air Sampling and
Stack Emissions Methods
A. Why is EPA proposing revisions to the
air sampling and stack emissions
methods?
B. Proposed Changes to Mercury
Thermometer Requirements in SW–846
Method-Defined Parameter Air Sampling
and Stack Emissions Methods
VII. Incorporation by Reference
VIII. State Authorization
A. Applicability of Proposed Rule in
Authorized States
B. Effect on State Authorization
IX. Statutory and Executive Orders Reviews
A. Executive Order 12866: Regulatory
Planning and Review and Executive
Order 13563: Improving Regulation and
Regulatory Review
B. Executive Order 13771: Reducing
Regulations and Controlling Regulatory
Costs
C. Paperwork Reduction Act (PRA)
D. Regulatory Flexibility Act (RFA)
E. Unfunded Mandates Reform Act
(UMRA)
F. Executive Order 13132: Federalism
G. Executive Order 13175: Consultation
and Coordination With Indian Tribal
Governments
H. Executive Order 13045: Protection of
Children From Environmental Health
Risks and Safety Risks
I. Executive Order 13211: Actions
Concerning Regulations That
Significantly Affect Energy Supply,
Distribution or Use
J. National Technology Transfer and
Advancement Act (NTTAA)
K. Executive Order 12898: Federal Actions
To Address Environmental Justice in
Minority Populations and Low-Income
Populations
I. General Information
A. Does this action apply to me?
The proposed rule to update the test
methods for determining if a liquid
waste is ignitable under the ignitability
characteristic may potentially affect any
entity (e.g., generator, laboratory) that
currently conducts flash point testing
using either SW–846 Method 1010A
(Pensky-Martens) or Method 1020B
(Setaflash). The rule may also affect any
entity (e.g., generator, laboratory,
combustor) that uses SW–846 air
sampling and stack emissions Methods
0010, 0011, 0020, 0023A, or 0051. EPA
does not expect the other parts of this
proposed action (i.e., changes to
aqueous alcohol exclusion, addition of
sampling guidelines for multiphase
mixtures, and technical edits) to affect
any entity because they do not create
new requirements or change existing
requirements.
The universe of facilities affected by
the proposed updates to the ignitability
test methods and SW–846 air sampling
and stack emissions methods includes:
(1) Commercial laboratories, (2) EPA
laboratories, and (3) state laboratories.
EPA identified 217 unique commercial
laboratories that conduct ignitability
testing under either Method 1010A or
1020. EPA identified an additional 18
commercial laboratories accredited to
conduct any of the air sampling and
stack emissions methods that would be
updated under this proposed rule, for a
total of 235 commercial labs affected by
the rule. These 235 total laboratories are
part of 177 unique firms, including
several large commercial laboratories
with multiple locations. EPA estimates
that the total number of laboratories,
including 20 state and nine federal
laboratories, potentially affected by this
rule is 264. The analysis used to identify
the potential universe for this proposed
rule can be found in EPA’s Regulatory
Impact Analysis of the Modernization of
Ignitable Liquid Determination Rule,
which is in the docket.
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00014 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12541
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
1
ASTM International (ASTM) is a nonprofit
organization, made up of producers, users,
consumers, government, and academia, that
develops and publishes consensus-based standards
(https://www.astm.org/).
This discussion is not intended to be
exhaustive but rather provides a guide
for readers regarding entities likely to be
regulated by this action. This discussion
lists the types of entities that EPA is
now aware could potentially be
regulated by this action. If you have
questions regarding the applicability of
this action to a particular entity, consult
the person listed in the
FOR FURTHER
INFORMATION CONTACT
section.
B. What action is the Agency taking?
First, EPA proposes to update the
flash point test methods required for
determining if a liquid waste is an
ignitable hazardous waste. Second, EPA
is proposing to codify existing guidance
regarding the regulatory exclusion in the
ignitable characteristic for aqueous
liquids containing alcohols and is
requesting comment on whether
additional changes may be warranted.
Third, EPA is proposing to codify
existing sampling guidance regarding
waste mixtures having multiple phases
when determining whether a waste
exhibits the ignitability characteristic.
Fourth, EPA is proposing to update
cross references to Department of
Transportation regulations and to
remove obsolete information. Finally,
EPA is proposing to provide alternatives
to the use of mercury thermometers in
the air sampling and stack emissions
methods in Test Methods for Evaluating
Solid Waste: Physical/Chemical
Methods (SW–846). Adding the option
of using non-mercury thermometers in
place of mercury thermometers would
provide the regulated community with
increased flexibility in their
implementation of these required test
methods. The use of alternatives to
mercury thermometers is consistent
with previous Agency actions and helps
achieve the Agency’s goal of minimizing
the use of mercury.
The EPA is proposing and requesting
comment on revisions to modernize the
ignitability flash point test methods
(Methods 1010A and 1020B) and air
sampling and stack emissions methods
(Methods 0010, 0011, 0020, 0023A, and
0051) to allow the use of non-mercury
thermometers. The Agency is also
proposing to update the ignitability
regulation (40 CFR 261.21) by codifying
guidance for aqueous alcohol solutions
and multiphase mixtures, as well as
making technical corrections. EPA
expects this proposed rulemaking to
improve hazardous waste identification,
reduce testing costs, improve laboratory
safety, and improve environmental
compliance, thereby enhancing
protection of human health and the
environment.
C. What is the Agency’s authority for
taking this action?
The authority to propose this rule can
be found in sections 1002, 1006, 2002,
3001–3009, 3013, and 3017 of the Solid
Waste Disposal Act (SWDA) of 1970, as
amended by the Resource Conservation
and Recovery Act (RCRA) of 1976, as
amended by the Hazardous and Solid
Waste Amendments of 1984 (HSWA), 42
U.S.C. 6901, 6905, 6912, 6921–6929,
6934, and 6938.
D. What are the incremental costs and
benefits of this action?
EPA prepared an economic analysis of
the potential costs and benefits
associated with this proposed action.
The Regulatory Impact Analysis of the
Modernization of Ignitable Liquid
Determinations Rule is available in the
docket. The proposed rule will modify
SW–846 test methods while also
retaining the current procedures to
provide entities increased flexibility.
For the purpose of the analysis, EPA
assumes that every facility that
currently conducts flash point testing:
(1) Is compliant with the current test
methods, (2) will adopt the updated test
methods if cost effective, and (3) will
continue to conduct flash point testing.
The analysis indicates that the rule, as
proposed, is projected to result in
annualized cost savings of about
$78,500 to $477,000 (based on a
discount rate of 7 percent). The net
present value of costs over 20 years is
estimated to be a cost savings of
$832,000 to $5 million (seven percent
discount rate). EPA’s analysis shows
qualitative benefits to human health and
the environment through the reduced
use of mercury thermometers.
II. Background
A. What is a hazardous waste?
Subtitle C of RCRA and its
implementing regulations establish a
cradle-to-grave regulatory management
scheme for certain solid wastes that
qualify as hazardous wastes. RCRA
defines solid waste as ‘‘any garbage,
refuse, sludge from a waste treatment
plant, water supply treatment plant, or
air pollution control facility and other
discarded material, including solid,
liquid, semisolid, or contained gaseous
material * * *.’’ (See RCRA 1004(27),
42 U.S.C. 6903(27).) EPA has further
defined the term solid waste for
purposes of its RCRA hazardous waste
regulations (40 CFR 261.2). To be
considered a hazardous waste, a
material first must be classified as a
solid waste. Under EPA’s regulations,
generators of solid waste are required to
determine whether their wastes are
hazardous wastes (40 CFR 262.11). A
solid waste is a hazardous waste if it
exhibits any of the four characteristics
of ignitability, corrosivity, reactivity, or
toxicity (40 CFR 261.20–.24), or is a
listed waste (40 CFR 261.30–.33). Listed
wastes include wastes from non-specific
sources, such as spent solvents; by-
products from specific industries; and
discarded, unused commercial chemical
products.
B. What is the hazardous waste
characteristic of ignitability?
The characteristic of ignitability (40
CFR 261.21) identifies solid waste as
hazardous based on the properties of the
waste that give it the potential to cause
harm to human health or the
environment through direct or indirect
fire hazard, including contributing to or
causing landfill fires. Waste that is
identified as hazardous pursuant to 40
CFR 261.21 has the EPA Hazardous
Waste Number of D001. Ignitable
hazardous waste (D001) is regulated to
minimize its opportunity to cause or
contribute to fires during routine waste
management activities. Solid wastes that
are regulated as ignitable hazardous
waste include: (1) Certain liquids with
flash points below 60 °C (140 °F); (2)
non-liquid substances that are capable,
under specified conditions, of causing
fire through friction, absorption of
moisture, or spontaneous chemical
changes and, when ignited, burns so
vigorously and persistently that they
create a hazard; (3) ignitable compressed
gases; and (4) oxidizers.
C. What is the regulatory history of the
ignitability characteristic?
The ignitability characteristic was
originally proposed in 1978 (43 FR
58945) with an objective of identifying
wastes that present a fire hazard due to
being ignitable under routine waste
disposal and storage conditions. The
ignitability characteristic was finalized
in 1980 when EPA promulgated the first
phase of regulations under Subtitle C of
RCRA to protect human health and the
environment from the improper
management of hazardous waste (45 FR
33066, May 19, 1980). These regulations
included 40 CFR part 261, which in
part, defined the ignitability
characteristic and incorporated by
reference ASTM
1
D 93–79 (Pensky-
Martens) and ASTM D 3278–78
(Setaflash) as the required tests for
ignitable liquid hazardous waste
determinations. In a 1981 revision, EPA
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00015 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12542
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
revised SW–846 Method 1010 to allow
the use of D 93–79 or D 93–80 (46 FR
35246, July 7, 1981).
ASTM standards D 3278–78, D 93–79,
and D 93–80 were the methods available
for flash point testing at the time of the
1980 and 1981 rulemakings. Since that
time, ASTM International (ASTM) has
updated D 93 and D 3278 multiple times
to improve the standards and
incorporate new technology. EPA
previously proposed to update the flash
point test methods for ignitability in the
2002 proposed Methods Innovation
Rule (67 FR 66252, Oct 30, 2002) by
replacing ASTM standard D 3278–78
with D 3278–96 and ASTM standards D
93–79 and D 93–80 with D 93–99c. In
that proposed rule, EPA also requested
comment on whether D 93–00 should
instead replace D 93–79 and D 93–80.
The public raised concerns that the
sampling procedures of the proposed
versions of D 93 may lead to a loss of
flammable volatile constituents from a
sample due to greater headspace in the
sampling container. The Agency made
the decision to not revise flash point
testing when the Methods Innovation
Rule was finalized in 2005, agreeing
with public comments that EPA further
study the changes in flash point testing
standards (70 FR 34550, June 14, 2005).
EPA later made corrections to the
ignitability characteristic to replace
obsolete references to DOT regulations
related to definitions of ignitable
compressed gases and oxidizers (see
July 14, 2006 Federal Register; 71 FR
40254). That final rule amended
§ 261.21 by revising paragraphs (a)(3)
and (a)(4) and adding notes 1 through 4
to the end of the section. No change was
made to § 261.21(a)(1). The current
language in § 261.21(a)(1) is
substantively the same as it was in 1980.
D. What is a flash point and how is it
measured?
The Kirk-Othmer Encyclopedia of
Chemical Technology defines a flash
point as the lowest temperature,
corrected to normal atmospheric
pressure (101.3kPa), at which the
application of an ignition source causes
the vapors of a liquid specimen to ignite
under the specific conditions of the test
(Solvents. Kirk-Othmer Encyclopedia of
Chemical Technology. 1–40). A flash
point can be measured using a
specifically designed apparatus
operated under specified procedures. In
general, these procedures involve
incrementally heating a liquid sample to
a specified temperature in an open or
closed cup and then exposing the
vapors above the liquid to a flame or
electric spark ignition source. The
person performing the test looks for a
flash caused by the vapor phase
igniting; if no flash is observed, the
sample is heated to a higher temperature
and the experiment is repeated. When
used for RCRA regulatory purposes, the
test is repeated until the temperature
surpasses 60 °C (140 °F) using specified
procedures and apparatuses to ensure
that accurate and precise waste
determinations are being made.
E. What flash point test methods does
EPA currently require?
EPA currently requires the use of one
of two flash point test methods when
making an ignitability hazardous waste
determination for liquid wastes, if
generator knowledge is not used. (For
more information on the use of
generator knowledge, see Agency
guidance, Waste Analysis at Facilities
that Generate, Treat, Store and Dispose
of Hazardous Wastes, available in the
docket.) The required test methods to
determine the method-defined
parameter for the flash point of ignitable
hazardous waste are SW–846 Methods
1010A and 1020B, which are listed in
40 CFR 260.11 and required by 40 CFR
261.21(a)(1). EPA requires the use of a
specific method to obtain a method-
defined parameter when the particular
procedures and/or equipment of that
method are necessary to achieve the
property measurement required by
regulation. Therefore, to determine
whether a liquid waste is ignitable
hazardous waste under RCRA (i.e., has
a flash point less than 60 °C (140 °F)),
its flash point must be assessed
according to the procedures and
instrumentation set forth in Methods
1010A or 1020B. While other methods
may exist that can measure the flash
point of a liquid waste, only the test
methods set forth in Methods 1010A or
1020B may be used for determining
whether a liquid waste is ignitable
under 40 CFR 261.21(a)(1). Because
using Method 1010A or 1020B yields
results that are driven by the particular
technical specifications in those
methods, the measures and outcomes
from these methods are known as
method-defined parameters, and their
required use in section § 261.21 can
only be amended through a regulatory
effort.
Method 1010A is a test method for
flash point measurement using a
procedure and instrumentation
commonly referred to as the Pensky-
Martens method. Method 1010A, or the
Pensky-Martens method, incorporates
by reference ASTM standards D 93–79
and D 93–80. The last two digits at the
end of these ASTM standards indicate
the year of publication for these
standards (i.e., 1979 and 1980,
respectively). ASTM standard D 93 is an
actively maintained standard under the
ASTM Committee D02 on Petroleum
Products, Liquid Fuels, and Lubricants.
The most recent update to the D 93
standard is D 93–16a, which was
published in 2016.
Alternatively, SW–846 Method 1020B
can be used for determining the
hazardous waste characteristic of
ignitability for liquids. Method 1020B is
a test method for flash point
measurement using the Setaflash, or
small-scale closed-cup, device and
method. Method 1020B incorporates by
reference ASTM standard D 3278–78,
which is maintained by the ASTM
Committee D01 on Paint and Related
Coatings, Materials, and Applications.
The last update to this ASTM standard
was in 1996. However, the standard was
reaffirmed in 2011 as ASTM D 3278–
96(2011).
In making an ignitable liquid
hazardous waste determination, either
the Pensky-Martens or the Setaflash
method may be used for most wastes.
The Pensky-Martens test is more
appropriate for liquids that are
nonhomogenous, form films, have high
viscosities, or are slurries because it
uses an instrument that can
mechanically mix wastes. The Setaflash
method, however, provides a practical
advantage of reduced sample size and,
therefore, reduced lab waste generation
when compared to the Pensky-Martens
method. Generators and laboratories
should choose to use the test method
that is most suitable to their needs.
F. What is the aqueous alcohol
exclusion?
The ignitability characteristic in
§ 261.21(a)(1) excludes ‘‘aqueous
solution[s] containing less than 24
percent alcohol by volume’’ from the
scope of liquids subject to § 261.21.
When EPA originally proposed the
ignitability characteristic in 1978, the
proposed rule did not contain an
exclusion for aqueous alcohols (43 FR
58945). Commenters on the 1978
proposed rule ‘‘argued that the
ignitability characteristic improperly
includes many liquid wastes such as
wine, latex paint and other water borne
coatings which contain low
concentrations of volatile organics such
as alcohol and will consequently exhibit
flash points below 100 °F but will not
sustain combustion because of the high
percentage of water present.’’
(Background Document for the
Characteristic of Ignitability, US EPA,
May 2, 1980, page 38.) In response, EPA
modified the ignitability characteristic
in the final rule with ‘‘an exclusion
similiar [sic] to that prescribed by DOT
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00016 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12543
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
2
Note that even if this waste stream falls within
the scope of the aqueous alcohol exclusion and,
thus, would not be regulated as an ignitable
hazardous waste, this waste stream could still be
regulated as a hazardous waste if it exhibits other
hazardous characteristics or is listed. In addition,
once a waste stream no longer meets the
requirements of the exclusion or is likely to not
meet the requirements during normal management
(e.g., the water or alcohol content changed), the
waste would be subject to regulation under the
ignitability characteristic.
3
A copy of this Question and Answer has been
placed into the docket for this proposal. A version
is also available at www.epa.gov/rcraonline, RCRA
Online Number 13548.
4
In developing this proposed rule, EPA reviewed
how the ignitability characteristic’s aqueous alcohol
exclusion related to the alcohol exclusion under
DOT’s Hazardous Materials Regulations (HMR). A
summary of DOT’s HMR’s exemption of alcoholic
beverages and aqueous solutions of alcohol has
been placed into the docket for reference.
5
This memorandum is available at https://
www.epa.gov/mercury/2008-memo-requiring-all-
epa-labs-phase-out-use-mercury-filled-
thermometers and in the docket.
6
This document is available at https://
www.epa.gov/sites/production/files/2015-10/
documents/nistuserfriendlyguide.pdf and in the
docket.
7
This report is available at https://
www.atsdr.cdc.gov/mercury/mercury_report.html
and in the docket.
8
See https://www.astm.org/SNEWS/SO_2008/
mercury_so08.html and the docket.
9
See http://www.mercuryconvention.org/.
[Department of Transportation] and
exempt from the ignitability
characteristic aqueous solutions with
alcohol concentrations of less than 24
percent by volume. This exclusion will
remove from the ignitability
characteristic such things as wine and
latex paint which flash at less than
100 °F but will not sustain combustion.’’
(ibid., 39.) Thus, the 1980 final rule
codified the following text in the
definition of ignitability at
§ 261.21(a)(1): ‘‘It is a liquid, other than
an aqueous solution containing less
than 24 percent alcohol by volume, and
has a flash point less than 60 °C
(140 °F).’’
2
(45 FR 33121; May 19, 1980.)
EPA later clarified the alcohol
exclusion in several ways. In the
preamble to a later rulemaking (55 FR
22543, June 1, 1990), EPA stated that
‘‘the term alcohol [in § 261.21(a)(1)]
refers to any alcohol or combination of
alcohols’’ and noted that ‘‘[i]f the
alcohol has been used for solvent
properties and is one of the alcohols
specified in EPA Hazardous Waste No.
F003 or F005, the waste must be coded
with these Hazardous Waste Numbers.’’
In addition, in 1992, the EPA clarified
that the ‘‘alcohol exclusion in 40 CFR
261.21(a)(1), however, is not limited to
those wastes mentioned in the May 19,
1980, Federal Register. It applies to all
aqueous solutions containing less than
24 percent alcohol, even if additional
non-alcoholic components are present.’’
(EPA Monthly Hotline Report, EPA530–
R–92–014g, July 1992, page 3.)
3
In that
clarification, EPA stated that the
‘‘alcohol exclusion for the ignitability
characteristic was adopted from the
Department of Transportation’s (DOT)
definition of ‘‘combustible liquids’’ in
49 CFR 173.115(b). The alcohol
exclusion in 49 CFR 173.115(b)(2)(ii)
applies to aqueous solutions containing
24 percent or less alcohol by volume
which contain no less than 50 percent
water. Since EPA originally intended to
be consistent with DOT regulations
when promulgating the alcohol
exclusion in § 261.21(a)(1), the 50
percent water stipulation may be
applied to the ignitability
characteristic.’’
4
Thus, for the purpose
of the ignitability characteristic in
§ 261.21(a)(1), EPA stated that
‘‘aqueous’’ means a ‘‘solution
continuing at least 50 percent water by
weight.’’ (ibid., 4.)
G. Why consider alternatives to mercury
thermometers in test methods?
Today, EPA is proposing to remove
the requirement to use mercury
thermometers in several EPA analytical
methods by revising the method or by
adding modern alternative methods that
may be used. Because of its unique
properties, elemental mercury has been
used in many applications, including
thermometers, fluorescent light bulbs,
and some electrical switches. However,
mercury from these devices can enter
the environment through breakage or
spills during use and during recycling
or disposal. Mercury is a potent
neurotoxin with a variety of well-
documented negative health effects. For
more information on the negative health
effects of mercury exposure, see https://
www.epa.gov/mercury/health-effects-
exposures-mercury#self.
Government agencies continue to
phase out the use of mercury devices,
including efforts by EPA (see 76 FR
2056, January 12, 2011; 77 FR 2456,
January 18, 2012; and the September 30,
2008 memorandum, Phasing Out
Mercury Filled Thermometers
5
), the
National Institute of Standards and
Technology (NIST) (see User-Friendly
Guidance on the Replacement of
Mercury Thermometers
6
), and the
Agency for Toxic Substances and
Disease Registry (ATSDR) (see report on
Children’s Exposure to Elemental
Mercury: A National Review of Exposure
Events
7
). Organizations, including
ASTM International (see ASTM and the
Mercury Initiative
8
) and the United
Nations Environment Programme
(UNEP) (see Minamata Convention
9
),
have also worked to phase out mercury
thermometer usage. EPA maintains
information on efforts to reduce
mercury exposures and to address
mercury pollution in the environment at
https://www.epa.gov/mercury. In the
majority of uses, mercury thermometers
can be replaced with safer, technically
appropriate, readily available non-
mercury temperature measurement
devices (Ripple and Strouse J. ASTM
International 2005).
III. Proposed Revisions to the
Ignitability Characteristic Flash Point
Test Methods
A. Why is EPA proposing new flash
point test methods for ignitable liquids?
Although the flash point test methods
currently required by § 261.21(a)(1)
provide accurate determinations of
whether a liquid waste is characteristic
for ignitability, these methods were
published about 40 years ago, and
newer technology is now available. As
explained in Section II.E. in this notice,
SW–846 Method 1010A currently
incorporates by reference ASTM
standards D 93–79 and D 93–80, which
are known as the Pensky-Martens
method. SW–846 Method 1020B
currently incorporates by reference
ASTM standard D 3278–78, otherwise
known as the Setaflash method. These
test methods represented technology
and best practices developed in 1978,
1979, and 1980. Since then, the ASTM
committees that maintain these
standards have updated these test
methods to incorporate modernized
technology and practices, but the RCRA
regulations still require the use of the
1978, 1979, and 1980 versions.
Due to the scientific and technological
advances over the last few decades,
these methods have become outdated
and their use presents several
challenges to the regulated community.
For instance, these standards require
mercury thermometers, which are being
phased out because of the
environmental health and safety
concerns of mercury. The Agency’s
mercury thermometer requirements
have become more difficult to meet as
organizations, such as NIST (NIST,
2011), discontinue calibration services
for mercury thermometers; consensus-
based bodies, such as ASTM (ASTM,
2008), phase out mercury thermometers
from their standards; and instrument
manufacturers phase out mercury
thermometers from commercially
available equipment. As part of its
efforts to reduce mercury usage and
release, and in the interest of providing
the regulated community with modern,
readily available options for
compliance, EPA has already revised
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00017 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12544
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
SW–846 methods that require the use of
mercury thermometers to allow for the
use of non-mercury-containing
temperature measuring devices (77 FR
2456, Jan 18, 2012; 79 FR 11228, Feb 27,
2014).
The decreased use of mercury
thermometers and new technology in
modern instrumentation combined with
the decreased availability of calibration
services limit commercially available
flash point devices that meet the current
EPA testing requirements for ignitable
waste. First, the flash point standards
required by EPA use reference materials
that, as EPA understands, are no longer
commercially available as certified
reference materials, such as para-xylene
for D 3278–78. Second, new
technologies, such as electric spark
ignition sources in place of flame
ignition sources, offer improved lab
safety and are available in modern
instruments. Third, the Agency believes
that new instruments may not be able to
increase temperature at the specified
rate (temperature ramping rate) in SW–
846 Method 1020B.
EPA is proposing to revise the
existing required Flash Point Test
Methods 1010A and 1020B by adding
modern consensus-based standards that
reflect the improvements and
modernization of flash point testing that
has occurred since 1978 to the methods
currently required by 261.21(a). EPA
understands that many generators and
laboratories already have
instrumentation capable of modern flash
point testing. Therefore, the proposed
update adds the flexibility of using
modern test methods, provides the
potential for cost savings, and enhances
the protection of human health and the
environment while providing equivalent
results (See Section III.D. for
information on how the proposed test
methods are equivalent to the currently
required test methods).
B. What test method is EPA proposing
to add to Method 1010A?
EPA is proposing to revise 40 CFR
261.21 and update Method 1010A to
Method 1010B to incorporate by
reference ASTM standard D 8175–18 as
an alternative to ASTM standards D 93–
79 and D 93–80 (Pensky-Martens
method) (see Table 1). The D 8175–18
standard is maintained by the ASTM
Committee D34 on Waste Management,
with whom the Agency worked to
modify the existing D 93–16 standard
for waste testing. The creation of the D
8175–18 standard utilized the existing
knowledge and practices of the flash
point testing community to develop a
standard specifically suited for flash
point testing of waste matrices.
The Agency initially considered
proposing to incorporate by reference
ASTM standard D 93–16 as a required
flash point test method. ASTM standard
D 93, has been updated numerous times
between 1980 and 2017. The 1979,
1980, 2016, and 2017 versions of D 93
all achieve the same fundamental
measurement; the newest versions
incorporate newer technology, provide
more detailed procedures, and include
quality control measures, such as
instrument verification using certified
reference materials. However, the D 93–
16 standard was written for the testing
of petroleum products, and EPA, after
reviewing the standard, had concerns
that the standard was not ideally suited
for flash point testing of waste forms.
The matrices of discarded chemicals,
lab wastes, liquids from emergency
response, free products, and other
wastes that might make up a waste
mixture are often more complex and
varied than petroleum products. The
Agency is concerned about the
appropriateness of some aspects of the
D 93–16 sampling procedures when
applied to waste analysis. The D 93–16
standards were developed primarily to
test the flash point of products while
RCRA testing requirements are often for
more complex mixtures. For example,
heating a sample to lower the viscosity
before placing it in the closed cup
device for measurement of the flash
point may produce results that are not
representative when testing waste
mixtures with relatively small
concentrations of volatile components
that easily ignite and readily evaporate
at elevated temperatures. The Agency
notes that the public raised similar
concerns in comments regarding the
Agency’s proposal to incorporate D 93–
99c by reference as part of the Methods
Innovation Rule (See comments by the
American Chemistry Council, EPA
Docket Number EPA–HQ–RCRA–2002–
0025). The D 93–16 standard is also
designed to measure petroleum
products in a temperature range from 40
°C to 370 °C. As the regulatory criteria
for flash point of ignitable liquids is 60
°C and below, EPA worked with ASTM
to modify the D 93–16 test procedure to
measure flash points of waste matrices
in a narrower temperature range and
closer to room temperature. The lower
but narrower temperature range
required for RCRA ignitability testing
also allows for a slower temperature
ramp rate in the method. The Agency
notes that it is possible that the lowest
temperature of the apparatus is
significantly higher than the actual flash
point of the sample. Some liquids such
as gasoline, pentane, hexane, natural gas
condensate, drip oil, etc. have flash
points below ¥20 C, the lower limit of
the small scale closed cup test method.
Conditions can exceed the fire point
(see ASTM D92) and a significant
enlargement of the test flame is
observed. In such situations, it is to be
concluded that the flash point is below
the range of the tester and hence below
60 C.
T
ABLE
1—S
UMMARY OF
C
URRENT AND
P
ROPOSED
SW–846 F
LASH
P
OINT
T
ESTS AND THE
ASTM S
TANDARDS
I
NCORPORATED BY
R
EFERENCE
ASTM
Standard
incorporated
by reference
Common name Status EPA SW–846
method
number
Publication
year
D 93–79 .......... Pensky-Martens ............................................. Current flash point test method used in
§ 261.21(a)(1). 1010A 1979
D 93–80 .......... Pensky-Martens ............................................. Current flash point test method used in
§ 261.21(a)(1). 1010A 1980
D 8175–18 ...... Pensky-Martens ............................................. Proposed modern, alternative flash point test
method. 1010B 2018
D 3278–78 ...... Setaflash, Small Scale Closed Cup ............... Current flash point test method used in
§ 261.21(a)(1). 1020B 1978
D 8174–18 ...... Setaflash, Small Scale Closed Cup ............... Proposed modern, alternative flash point test
method. 1020C 2018
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00018 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12545
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
10
Repeatability and Reproducibility are terms
defined by ASTM and other organizations.
Repeatability is precision determined from multiple
test results by a single, well trained operator in a
single lab with one set of equipment.
Reproducibility is precision determined from
multiple tests in several laboratories. See ASTM
E177–14 for more information.
C. What test method is EPA proposing
to add to Method 1020B?
EPA similarly worked with ASTM to
modify the current version of the small-
scale closed-cup flash point test. EPA is
proposing to revise § 261.21 and update
Method 1020B to Method 1020C,
incorporating by reference the resulting
ASTM standard D 8174–18 as an
alternative to ASTM standard D 3278–
78 (Setaflash method) (see Table 1). The
D 8174–18 standard is an updated
version of the D 3828–16a standard that
has been modified to be more
appropriate for waste testing. EPA first
considered incorporating by reference D
3278–96(2011), which is the most
current version of the standard that is in
Method 1020B. However, this standard
does not use the most modern
technology available for Setaflash
closed-cup testing, having been last
updated in 1996 (and last reaffirmed in
2011). As ASTM has multiple standards
for closed-cup flash point testing, EPA
also considered the suitability of ASTM
standards D 7236–16 and D 3828–16a.
Due to EPA’s understanding that D 3828
is a preferred method in the analytical
community, EPA focused on ASTM
standard D 3828–16a as a new test for
ignitable liquids. After further review of
ASTM D 3828–16a standard, the Agency
identified concerns with the sampling
procedures similar to the Agency’s
concerns with D 93–16 as stated in
Section III.B. The sampling procedures
in 3828–16a are refined and optimized
for petroleum products. Waste matrices
can be mixtures of a wide variety of
chemical compounds with varying
physical properties and may present
sampling challenges not often found in
petroleum products. As a result, EPA
worked with ASTM to adapt the
standard to waste samples.
Additionally, EPA was interested in a
testing procedure that minimized
sampling requirements and waste
generation. The use of a finite flash
method would require that samples
with unknown flash point temperatures
be measured in a series of tests until a
flash was detected. Each test in the
series would require a new sample be
placed in the tester, increasing the
amount of sample required for analysis
and waste generated by testing.
Therefore, EPA worked with ASTM to
develop a modified version of ASTM
standard D 3828–16a that also includes
a non-mandatory ramp test. This ramp
test procedure (found in the appendix of
D 8174–18) can be used to determine an
estimated flash point when working
with an unknown sample. The
estimated flash point can then be used
to perform the finite flash test
procedure, limiting the total number of
tests needed when the expected flash
point of a sample is not known.
D. How are the proposed test methods
equivalent to the currently required test
methods?
Technical changes between the
currently required SW–846 Methods
1010A and 1020B and the proposed test
methods include the allowance for an
automatic method with electronic flash
point detection, the option to use a
flame ignition source or an electric
ignition source, and use of non-mercury
temperature devices. The changes in
instrumentation that have occurred over
time as new technology was developed
present opportunities for improvements
to a method but also may affect
precision, accuracy, or bias of an
instrument or method. In the process of
adapting these new technologies, ASTM
and other organizations have conducted
a number of studies to verify that these
technological changes present
equivalent testing results, as discussed
below.
The use of automated instrumentation
for flash point testing has been a widely
accepted practice for decades. In 1992,
ASTM completed a round robin study
(see Research Report S15–1008 in
docket) using ASTM standards D 92 and
D 93 to determine the precision and
accuracy of automatic and manual flash
point instruments. This round robin
study found no statistical difference
between the reproducibility variances of
automatic and manual Pensky-Martens
flash point methods.
The use of electric ignition sources in
flash point testing improves lab safety.
The Energy Institute funded a round
robin study to determine the precision
for ASTM D 3828–9 using both gas and
electric igniters (see Energy Institute
Research Report, August 15, 2010 in
docket). The round robin study found
that while there was bias between the
electric and gas ignition sources, the
bias was small relative to the
repeatability of the method. ASTM took
this information into consideration and
decided to publish a combined
precision applicable to both gas and
electric ignitors for ASTM standard D
3828.
Both of the new ASTM standards that
will be incorporated by reference, D
8175–18 and D 8174–18, allow for the
use of temperature measuring devices
that are either digital or liquid-in-glass.
The digital temperature measuring
devices and liquid-in-glass
thermometers must meet the
specifications listed in Annex A1 and
A2 of D 8175–18 and Annex A4 of D
8174–18. These performance-based
specifications may allow for the use of
mercury-containing thermometers but
do not require them. The performance
requirements of temperature
measurement devices are set by
manufacturers to meet certification
standards set by NIST and other
standards organizations. The use of
calibrated and certified non-mercury
temperature measurement devices in
flash point testing is expected to
provide equivalent results (See User
Friendly Guidance on the Replacement
of Mercury Thermometers from NIST/
EPA in docket).
The changes in instrumentation to
incorporate new technology are already
reflected in the modern versions of the
ASTM standards that are currently
required by EPA for flash point testing
pursuant to 261.21 (e.g., modern
versions of D 93–79, such as D 93–16a,
have electric ignition sources). The
repeatability and reproducibility of the
modern standards are similar to that of
the standards currently required by
EPA.
10
This similarity, for the purposes
of flash point testing, indicates that the
results from either test method should
be similar.
For example, ASTM standard D 93–80
lists a repeatability of 2 °C and a
reproducibility of 3.5 °C for flash point
measurements of 104 °C and under. For
modern versions of D 93, repeatability
and reproducibility are dependent upon
the flash point temperature measured.
Therefore, using EPA’s regulatory value
for flash point of 60 °C in the
temperature-dependent equation given
by ASTM D 93–16, repeatability is 1.74
°C and reproducibility is 4.26 °C. ASTM
standard D 3278–78 gives a repeatability
of 1.7 °C and a reproducibility of 3.3 °C.
D 3278–96(11), which is the modern
version of D 3278–78, lists a
repeatability of 1.7 °C and a
reproducibility of 3.3 °C. The similar
values for repeatability and
reproducibility in the modern standards
and the 1978 to 1980 standards that EPA
currently requires shows that the
accuracy of these methods has remained
relatively unchanged despite the
adoption of new technology into the
standard as discussed above.
These precision and accuracy
statements from ASTM are based on
testing relatively pure reference
chemicals. To confirm these results for
more complex waste forms (e.g., those
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00019 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12546
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
consisting of multiple components and
multiple phases), a single lab study was
conducted. In ASTM standards D 8175–
18 and D 8174–18, a single lab study
using simulated waste matrices
determined repeatability for these
standards. The simulated waste matrices
were single phases consisting of an
equal volume mixture of xylenes and 1-
butanol, a mixture (by volume) of 60%
1-butanol and 40% n-decane, a mixture
(by volume) of 70% n-decane and 30%
n-undecane, and a mixture (by volume)
of 10% acetone and 90% n-heptane. A
multiphase mixture (by volume) of 50%
diesel, 47.5% water, and 2.5% acetone
was also studied (see D 8175–18 and D
8174–18 in the docket for specific
results). Based on these studies, D 8175–
18 repeatability is between 0.88 °C and
2.26 °C for the five samples tested. D
8174–18 repeatability is between 0.88 °C
and 2.34 °C for the five waste forms
tested. The repeatability values of D
8175–18 and D 8174–18 are consistent
with the stated repeatability of the
ASTM standards currently required by
SW–846 Methods 1010A and 1020B
(i.e., ASTM standards D 3278–78, D 93–
79, and D 93–80). EPA understands that
future updates to ASTM standards D
8175–18 and D 8174–18 will have more
robust precision and accuracy values
when ASTM completes interlaboratory
validation of the methods. EPA will
update the regulation or revisit the
accuracy of these test methods, if
necessary.
E. Why is EPA not removing the
currently required flash point test
methods?
ASTM standards D 93–79, D 93–80,
and D 3278–78 remain technically
acceptable methods for determinations
of flash point for ignitable liquids. The
Agency strongly encourages generators
and laboratories to use alternatives to
mercury thermometers whenever
possible but is also proposing flexibility
by not requiring that existing equipment
be modified or replaced to remove
mercury thermometers already in use.
The Agency anticipates that domestic
and international efforts to reduce
mercury usage, the environmental
benefits of removing mercury from the
workplace, and the economic benefits
from reduced testing costs will result in
generators and laboratories adopting the
new methods over time. This shift
toward using the new methods will
result in the reduction and eventual end
of mercury thermometer use in flash
point testing as part of the normal
process of upgrading or replacing
laboratory equipment.
The Agency is interested in input
from the public on whether it would be
more appropriate to remove the
incorporation by reference of D 93–79,
D 93–80, and D 3828–78 from SW–846
and 40 CFR 261.21 at this time. The
SW–846 Test Methods program states a
preference for the regulated community
to use the most up-to-date version of
SW–846 methods. However, to provide
flexibility, both the current and
proposed methods would need to be
specified in the regulation. By leaving
ASTM standards D 93–79, D 93–80, and
D 3278–78 incorporated by reference
within SW–846 Methods 1010 and 1020
and the ignitability regulation, the
Agency intends to provide the regulated
community the time it needs to
transition between the old and new test
standards. The Agency may remove
ASTM standards D 93–79, D 93–80, and
D 3278–78 from SW–846 Methods 1010
and 1020 and the ignitability regulation
in a future update.
IV. Codification of Guidance Into the
Ignitability Characteristic
A. Aqueous Alcohol Exclusion
1. Why is EPA proposing a revision to
the aqueous alcohol exclusion?
As part of its effort to update the
ignitability methods, the Agency
reviewed the exclusion for aqueous
solutions containing ignitable alcohols
to determine if the exclusion should be
revised. Since 1980, questions regarding
the scope of the exclusion have been
raised. As discussed in more detail in
Section II.F. of this notice, EPA has
provided clarification by interpreting
the exclusion to include any alcohol or
combination of alcohols (except if the
alcohol has been used for its solvent
properties and is one of the alcohols
specified in EPA Hazardous Waste No.
F003 or F005) that contains less than 24
percent alcohol by volume, even if
additional non-alcoholic components
are present, and at least 50 percent
water by weight.
EPA has since become aware that the
aqueous alcohol exclusion may
inadvertently exclude certain wastes
from the ignitibility characteristic—
aqueous liquids with small amounts of
alcohol, where these wastes are
ignitable due primarily to non-alcoholic
components—contrary to the intent of
the exclusion. For example, the
exclusion may apply to an aqueous
waste stream that contains a small
concentration of an ignitable alcohol
and a large concentration of an ignitable
non-alcoholic component. This waste
would be excluded from the ignitability
characteristic despite potentially
exhibiting the same hazards as ignitable
wastes that do not fall within the scope
of the exclusion.
EPA is currently unaware of existing
mismanagement or damage cases
resulting from this interpretation, and it
may only affect a small number of
(currently unknown) waste streams. The
Agency solicits information on the
experience of the regulated community,
state authorized programs, and others in
implementing this provision of the
ignitability characteristic (See Section
IV.A.3. in this notice).
2. What are the proposed changes to the
aqueous alcohol exclusion?
Due to questions received about the
alcohol exclusion under the RCRA
hazardous waste ignitibility
characteristic, EPA wants to use this
opportunity to clarify the exclusion’s
scope by proposing to codify the
existing guidance into the regulatory
text. Specifically, EPA is proposing to
revise the aqueous alcohol exclusion
from ‘‘other than an aqueous solution
containing less than 24 percent alcohol
by volume’’ to ‘‘other than a solution
containing less than 24 percent of any
alcohol or combination of alcohols
(except if the alcohol has been used for
its solvent properties and is one of the
alcohols specified in EPA Hazardous
Waste No. F003 or F005) by volume and
at least 50 percent water by weight.’’
This proposed change removes the term
‘‘aqueous’’ from § 261.21(a)(1), which is
currently undefined in the RCRA
hazardous waste regulations, and
specifies what percentage of water
defines the scope of this exclusion. The
Agency notes that the water content of
a waste is not a method-defined
parameter and more than one method or
procedure may be appropriate for
measuring the water content of a
sample. Existing SW–846 methods for
water quantification include EPA SW–
846 Methods 9000 and 9001. An analyst
should choose the most appropriate
method for measuring water content
based on the physical and chemical
properties of their waste.
Codifying the guidance into the
regulatory text would provide clarity
and certainty for the regulated
community and will remove the need
for generators and laboratories or
managers of waste to rely on multiple
documents to understand the intended
scope of the alcohol exclusion.
Today’s proposed action would have
no effect on 40 CFR 403.5(b)(1), which
prohibits ‘‘pollutants which create a fire
or explosion hazard in the POTW
[publicly owned treatment work],
including, but not limited to,
wastestreams [sic] with a closed cup
flash point of less than 140 degrees
Fahrenheit or 60 degrees Centigrade
using the test methods specified in 40
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00020 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12547
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
11
EPA evaluated whether the aqueous alcohol
exclusion in §261.21 should apply to 40 CFR
403.5(b)(1) and concluded that extending the
exclusion to 40 CFR 403.5(b)(1) is not appropriate.
(July 24, 1990 Federal Register; 55 FR at 30086).
‘‘POTW collection systems are an ideal
environment for generation of flammable/ignitable
atmospheres . . . allowing an exemption from the
flash point prohibition for aqueous solutions
containing less than 24 percent alcohol by volume
would not sufficiently protect POTWs.’’ (ibid.)
12
Letter dated November 20, 2012 from Betsy
Devlin, USEPA, to Gary Jones, Printing Industries
of America, available at www.epa.gov/rcraonline
(RCRA Online Number 14834). A copy of this letter
is available in the docket to today’s proposed rule.
CFR 261.21’’ with no exemption for
aqueous alcohol solutions (July 24, 1990
Federal Register; 55 FR 30082).
11
Any
revisions made to the aqueous alcohol
exclusion in § 261.21(a)(1) from this rule
would not change its inapplicability to
40 CFR 403.5(b)(1).
3. Solicitation of public input on other
changes to the aqueous alcohol
exclusion for ignitability
Because the aqueous alcohol
exclusion could be interpreted to be
more broadly applicable than originally
intended (See Section IV.A.1. in this
notice), EPA is seeking input on
whether any additional revisions should
be made to the aqueous alcohol
exclusion in § 261.21(a)(1). The Agency
is interested in the experiences of state
authorized programs that manage
excluded aqueous alcohols as solid
waste and whether state programs have
more stringent requirements. The
Agency is also interested in input from
waste generators, laboratories, and other
members of the public who may have
information regarding the specific
hazards, or lack thereof, of managing
waste streams pursuant to the current
exclusion. This information might
include: How much waste is generated
and managed under the exclusion for
aqueous alcohol solutions, how specific
waste is currently managed, what waste-
specific or industry-specific
management standards or established
practices for solutions of aqueous
alcohol waste already exist, what waste
forms are not currently excluded but
may warrant exclusion due to a lack of
risk to human health or the
environment, what specific waste forms
may currently be excluded despite
presenting risks to human health or the
environment, and any examples of
waste mismanagement, damage, or
injury resulting from waste managed
under the aqueous alcohol exclusion.
This information may help identify
appropriate revisions to the aqueous
alcohol exclusion for ignitable liquids to
limit the exclusion to its original intent.
Possible revisions to the aqueous
alcohol exclusion could include
explicitly identifying specific waste
streams in the regulation to which the
exclusion would apply to remove the
uncertainty regarding the current scope
of the exclusion and narrowing the
types of alcohol that would qualify for
the aqueous alcohol exclusion. Other
considerations could include adding a
minimum alcohol content as a
requirement for excluded wastes to
better target potential waste streams that
flash primarily from their alcoholic
components or adding to or improving
the existing criteria a waste must meet
to be eligible for the exclusion (e.g.,
raise the minimum water content for
aqueous alcohol solutions) to decrease
the likelihood that a liquid waste
excluded from the ignitability
characteristic would be able to sustain
combustion or otherwise contribute to
an ongoing fire. The Agency seeks
information that can be used to
determine appropriate revisions to the
aqueous alcohol exclusion.
B. Multiphase Testing
1. Why is the Agency proposing a
revision to codify sampling guidance for
multiphase wastes?
The Agency has received questions in
the past on sampling wastes that are
multiple phases or may become
multiple phases during normal
management. The proposed and current
test methods for ignitability contain
instructions and procedures specific to
that ASTM standard. The Agency is
proposing to add new language to
261.21(a) to clarify that EPA’s existing
sampling procedures for multiphase
samples would be applicable to all
liquid wastes tested under 261.21.
Existing guidance from the Agency
states that multiphase mixtures should
be separated so that each phase is
analyzed individually (discussed further
below).
2. Proposed Codification of Guidance
for Multiphase Waste Sampling
The Agency is proposing to add a new
paragraph to § 261.21(a) that clarifies
how to properly test multiphase wastes
containing multiple liquid(s) with or
without solids for ignitability
determinations. This added language
would codify EPA’s long-standing
sampling guidance for multiphase
wastes, which are wastes that, due to
differences in density (e.g., oil/water) or
physical form (e.g., solid/liquid),
separate into two or more phases. EPA’s
long-standing sampling guidance states
that for multiphase mixtures, a
generator and laboratory should
separate the sample into all of its
different solid and/or liquid phases, to
the extent practicable, and analyze each
one individually in accordance with
§ 261.21(a) to determine whether that
phase exhibits the characteristic of
ignitability. However, care should be
taken to avoid loss of volatiles during
separation, and it may not be possible
to remove solids in all multiphase
wastes. If the individual phases cannot
be separated without an appreciable loss
of volatiles such that the ignitability test
results may be affected, then the
multiphase waste should be tested for
flash point as a whole.
The Agency notes that some waste
mixtures may initially be one phase
upon generation and later separate into
two or more phases during the course of
normal management. The requirement
to make hazardous waste
determinations upon generation and at
any time during the course of
management (including if phase
separation occurs) is already clearly
stated in 40 CFR 262.11(a). ‘‘The
hazardous waste determination for each
[RCRA] solid waste must be made at the
point of waste generation, before any
dilution, mixing, or other alteration of
the waste occurs, and at any time in the
course of its management that it has, or
may have, changed its properties as a
result of exposure to the environment or
other factors that may change the
properties of the waste such that the
RCRA classification of the waste may
change.’’ This policy was reaffirmed in
the hazardous waste generator proposed
and final rules (80 FR 57938 and 81 FR
85751).
EPA’s existing guidance on
multiphase mixtures, which applies at
initial generation and during the course
of normal management, as applicable, in
SW–846 states to break up and separate
phases when possible (SW–846 Chapter
2, pp 8–9). For example, the Agency has
explained that a hazardous waste
determination is required for both
phases of a multiphase liquid and that
the RCRA sampling protocol called the
COLIWASA (Composite Liquid Waste
Sampler, ASTM D–5495), found in
Chapter Nine of EPA’s waste testing
guidance, ‘‘Test Methods for Evaluating
Solid Waste (SW–846),’’ can be used for
this purpose.
12
The proposed regulatory
language in this notice would clarify
that multiphase wastes should be
separated out into its different liquid
and/or solid phases, to the extent
possible, before then testing each
individual phase for ignitability in
accordance with § 261.21.
Related to this issue, EPA notes that
determining that a waste contains liquid
and separating liquid from solid may be
relatively straightforward through
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00021 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12548
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
observation, decanting, pipetting, or
simple gravity filtration (i.e., EPA
Method 9095, Paint Filter Liquids Test
or PFLT). However, confirming that a
waste does not contain liquid might not
be possible using these techniques for
some wastes. In 1993, the Agency
proposed Update II to SW–846, which
included modified language in SW–846
to state that the pressure filtration
technique specified in SW–846 Method
1311 (Toxicity Characteristic Leaching
Procedure or TCLP; see Section 7.1.1)
should be used to determine if a waste
contains a free liquid as part of making
hazardous waste characteristics
determinations such as ignitability or
corrosivity (August 31, 1993 Federal
Register; 58 FR 46052). The Agency did
not finalize this proposed modification
due to commenters’ concerns that the
proposed action would discourage the
use of Method 9095 (PFLT) in
demonstrating that a free liquid exists.
In the preamble to the final rule, EPA
clarified that the pressure filtration
technique should be used to definitively
determine that a free liquid did not exist
(January 13, 1995 Federal Register; 60
FR 3089). EPA stated,
‘‘The definitive procedure for determining
if a waste contains a liquid for the purposes
of the ignitability and corrosivity
characteristics is the pressure filtration
technique specified in Method 1311.
However, if one obtains a free liquid phase
using Method 9095, then that liquid may
instead be used for purposes of determining
ignitability and corrosivity. However, wastes
that do not yield a free liquid phase using
Method 9095 should then be assessed for the
presence of an ignitable or corrosive liquid
using the pressure filtration technique
specified in Method 1311.’’ (60 FR 3092,
January 13, 1995).
EPA also stated that it may re-propose
modifying its guidance in Chapter 7 to
reflect its stated position. Therefore, we
are requesting comment on adding this
language—which reflects EPA’s position
on determining free liquids—to SW–846
as guidance. Finally, with regard to
separating multiphase wastes for
purposes of testing, we note that
Method 9095B or the pressure filtration
technique in Method 1311 can be used
to remove solids in multiple phase
mixtures, whenever practical.
V. Additional Corrections to § 261.21
A. What are the proposed changes to the
definition of ignitable compressed gas in
§ 261.21(a)(3)(ii)?
As part of its effort to modernize and
update the RCRA ignitability
characteristic regulations in § 261.21,
the Agency is proposing corrections to
the ignitable compressed gas definitions
in § 261.21(a)(3)(ii), where EPA has
determined that particular Department
of Transportation (DOT) regulations
originally relied upon by EPA have
subsequently changed, or certain
guidance is no longer available.
First, EPA is proposing to update
§ 261.21(a)(3)(ii)(A) to replace outdated
references to the Bureau of Explosives
and DOT. The current EPA regulation at
§ 261.21(a)(3)(ii)(A) establishes that a
waste compressed gas is ignitable under
RCRA when certain flammability
concentration criteria are met, as
determined ‘‘using a test acceptable to
the Bureau of Explosives and approved
by the director of the Pipeline and
Hazardous Materials Technology, U.S.
Department of Transportation’’.
However, subsequent to the EPA’s
original promulgation of this provision,
DOT modified their regulations to
require ASTM standard E 681–85 or
‘‘other equivalent method approved by
the [PHMSA] Associate Administrator’’
as an approved test for this purpose (55
FR 52433). See 49 CFR 173.115(a). EPA
also notes that the Bureau of Explosives
is no longer the delegated authority
from DOT to determine this testing
requirement. (See communications with
Bureau of Explosives in the docket to
this proposed rule.) Therefore, EPA is
proposing to revise § 261.21(a)(3)(ii)(A)
to specify the ASTM standard E 681–85
as the approved test for determining
whether any waste that is an ignitable
compressed gas exhibits the RCRA
ignitability characteristic, and to remove
reference to the Bureau of Explosives as
an approving agency for sampling and
test methods. Consistent with the
current DOT regulations, EPA is also
proposing to correct in its own
regulations the reference identifying the
agency responsible for approving other
tests as equivalent for this purpose, by
adding the phrase ‘‘approved by the
Associate Administrator, Pipeline and
Hazardous Materials Safety
Administration, U.S. Department of
Transportation.’’
EPA is also proposing to revise
§ 261.21(a)(3)(ii)(B)–(D) to align with the
existing DOT regulations for flammable
gases. Paragraphs (B), (C) and (D) in
§ 261.21(a)(3)(ii) reference ‘‘Flame
Projection Apparatus,’’ ‘‘Open Drum
Apparatus,’’ and ‘‘Closed Drum
Apparatus,’’ all of which are described
as methods from the Bureau of
Explosives. EPA inquired with the
Bureau of Explosives about the
continued availability of these test
methods and found that the methods
were unavailable. (See correspondence
with the Bureau of Explosives in the
docket to this proposed rule.) In 1980,
the Agency incorporated these Bureau
of Explosives test methods into its
RCRA regulations to be consistent with
how flammable gases were defined by
DOT requirements. (See 45 FR 33108,
May 19, 1980 Federal Register; see also
Ignitability Background Document, U.S.
EPA, May 2, 1980 in the docket to this
proposed rule.) However, as discussed
earlier, DOT subsequently updated their
definition and testing requirements.
Therefore, the Agency is proposing to
update the definition of ignitable
compressed gas within
§ 261.21(a)(3)(ii)(B)–(D), by removing
references to Bureau of Explosives
methods, and to mirror the definition
and testing that DOT now requires. This
change will allow generators to
determine if their waste meets the
definition of an ignitable compressed
gas by determining if it meets the
definition of a Division 2.1 flammable
gas or a flammable aerosol (see 49 CFR
173.115(a) and (l)).
EPA believes that these updates are
necessary to ensure that the RCRA
definition reflects the current DOT
regulations for evaluating ignitable
compressed gases, consistent with
EPA’s longstanding approach to
incorporate certain DOT requirements
when establishing definitions (and
associated test methods) that reflect
routine waste management conditions
for these types of wastes.
B. What are the proposed changes to
§ 261.21(a)(4)(i)(A)?
In 40 CFR part 261, EPA is amending
this paragraph to read, ‘‘The material
meets the definition of a Division 1.1,
1.2, or 1.3 explosive, as defined in
§ 261.23(a)(8), in which case it must be
classed as an explosive.’’
Currently, § 261.21(a)(4)(i)(A)
references ‘‘a Class A explosive or a
Class B explosive.’’ The terms Class A
and B explosives came from the
classification system for explosives used
by DOT before 1991. However, DOT
revised its classification system for
explosives, based on the United Nations
Recommendations on the Transport of
Dangerous Goods, as part of a final rule
issued on December 21, 1990 amending
the Hazardous Materials Regulations (55
FR 52402). The new system replaced the
use of explosive classes A, B, and C
with the classification codes of 1.1, 1.2,
1.3, and 1.4 (49 CFR 173.53). EPA
issued a direct final rule on March 18,
2010 that, in part, incorporated these
changes into the RCRA hazardous waste
regulations. (75 FR 12989). This direct
rule amended 40 CFR 261.23(a)(8) to
read, ‘‘It is a forbidden explosive as
defined in 49 CFR 173.54, or is a
Division 1.1, 1.2 or 1.3 explosive as
defined in 49 CFR 173.50 and 173.53.’’
(75 FR 13002). Before this revision, 40
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00022 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12549
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
CFR 261.23(a)(8) referenced DOT’s
regulations addressing Class A
explosives and Class B explosives.
However, as the preamble to the rule
pointed out, ‘‘these cross-references are
out of date with the current DOT
regulations, and the referenced sections
either no longer exist or no longer
address these explosives. This change
modifies the rule to provide the correct
citations.’’ (75 FR 12993). Section
261.21(a)(4)(i)(A) was overlooked by the
2010 EPA rulemaking, and this
proposed change corrects that by
updating § 261.21(a)(4)(i)(A) with the
correct references.
C. What are the proposed changes to the
notes section of § 261.21?
EPA proposes to delete the four notes
at the end of 40 CFR 261.21, which are
outdated or unnecessary to
understanding the regulation.
EPA intends to delete Note 1 because
the Bureau of Explosives will no longer
be the source for the methods identified
in 261.21(a)(3)(ii)(B)–(D). The current
language for Note 1 states that a
‘‘description of the Bureau of
Explosives’ Flame Projection Apparatus,
Open Drum Apparatus, Closed Drum
Apparatus, and method of tests may be
procured from the Bureau of
Explosives.’’
EPA proposes to delete Notes 2 and 3.
Notes 2 and 3, respectively, state that as
part of a U.S. Department of
Transportation (DOT) reorganization,
the Office of Hazardous Materials
Technology (OHMT), which was the
office listed in the 1980 publication of
49 CFR 173.300 for the purposes of
approving sampling and test procedures
for a flammable gas, and the Research
and Special Programs Administration
(RSPA), which was the office listed in
the 1980 publication of 49 CFR 173.151a
for the purposes of determining that a
material does not present a hazard in
transport, ceased operations on
February 20, 2005. OHMT and RSPA
programs have moved to the Pipeline
and Hazardous Materials Safety
Administration (PHMSA) in the DOT.
This historical information is no longer
necessary to understanding the
regulation.
EPA also proposes to delete Note 4.
Note 4 was added in a 2006 EPA
rulemaking to provide referential
information to the change made to 40
CFR 261.21(a)(4) in the same action (71
FR 40254). Before the 2006 rule, 40 CFR
261.21(a)(4) incorporated by reference
the DOT regulation that defined an
oxidizer, 49 CFR 173.151. In 1990, DOT
revised its regulations governing
transportation of hazardous materials
(55 FR 52402), including 49 CFR
173.151. However, 40 CFR 261.21(a)(4)
retained the original DOT definition of
an oxidizer, causing the DOT section it
referenced to become irrelevant after
1990. EPA’s 2006 final rule replaced the
obsolete DOT reference in 40 CFR
261.21(a)(4) with the actual language
from 49 CFR 173.151 as it existed at the
time 40 CFR 261.21 was finalized in
1980. Note 4 states that ‘‘[t]he DOT
regulatory definition of an oxidizer was
contained in § 173.151 of 49 CFR, and
the definition of an organic peroxide
was contained in paragraph 173.151a.
An organic peroxide is a type of
oxidizer.’’ EPA proposes to remove Note
4 in this rulemaking to avoid possible
confusion, particularly because it can be
difficult to obtain copies of the CFR
from 1980.
VI. Revision to Mercury Thermometer
Requirements in the Air Sampling and
Stack Emissions Methods
A. Why is EPA proposing revisions to
the air sampling and stack emissions
methods?
Earlier in this action, EPA proposed to
modernize flash point determinations
for ignitable liquids by revising Methods
1010A and 1020B to adopt modern
consensus-based standards that allow
flexibility in temperature measurement
devices (see Section III.A.). Similarly,
EPA is proposing to update the SW–846
air sampling and stack emissions
methods that use mercury thermometers
and are method-defined parameters.
These methods are Methods 0010, 0011,
0020, 0023A, and 0051. This update
would provide current users of these
methods the flexibility to use alternative
temperature-measuring devices instead
of the currently required mercury
thermometers. The current users of
Methods 0010, 0011, 0020, 0023A, and
0051 would be able to continue using
mercury thermometers if desired. While
the test methods for flash point of
ignitable liquids and test methods for air
sampling and stack emissions methods
are unrelated in the hazard and matrix
of waste they analyze, the underlying
rationale and environmental benefits of
providing the flexibility to use
alternatives to mercury thermometers
are the same. As a result, EPA is
proposing these method revisions in the
same action. See Section II.G. above for
more information on the effects of
mercury on human health and the
environment.
B. Proposed Changes to Mercury
Thermometer Requirements in SW–846
Method-Defined Parameter Air
Sampling and Stack Emissions Methods
EPA has identified five SW–846
method-defined parameter test methods
for air sampling and stack emissions
methods that require the use of mercury
thermometers: Methods 0010, 0011,
0020, 0023A, and 0051 (see Section
VI.A.). These sampling methods cover
emissions from stationary sources, such
as hazardous waste incinerators and
boilers and industrial furnaces. Many of
these sampling methods are
modifications of, or are similar to, EPA
Method 5 of Appendix A–3 of 40 CFR
60, Determination of Particulate Matter
Emissions from Stationary Sources. For
Method 5, EPA proposed (77 FR 1130,
Jan 9, 2012), and finalized (79 FR 11228,
Feb 27, 2014), the use of alternative
mercury-free thermometers if the
thermometers are, at a minimum,
equivalent in terms of performance or
are suitably effective for the specific
temperature measurement application.
EPA is proposing to add similar
language, where appropriate, in SW–846
Methods 0010, 0011, 0020, 0023A, and
0051. The removal of the requirement to
use mercury thermometers does not
change the underlying technology of the
methods. Therefore, in accordance with
the SW–846 methods policy statement,
the method numbers and letters are not
being revised due to these changes (see
https://www.epa.gov/hw-sw846/policy-
statement-about-test-methods-
evaluating-solid-waste-
physicalchemical-methods). The
Agency anticipates that the addition of
mercury thermometer alternatives to
these methods (i.e., the mirroring of
changes made to regulatory
requirements under Method 5) should
result in a minimal impact to the
regulated community. For example,
analytical laboratories that offer these
air sampling and stack emissions
methods also likely offer Method 5
testing, which already allows for non-
mercury thermometer usage. Labs that
have non-mercury thermometers for
calibrating Method 5 should recognize
the benefits of reduced mercury
thermometer usage while incurring no
additional costs. Alternatively,
laboratories may continue using
mercury thermometers in the updated
methods (see Section III.E.).
VII. Incorporation by Reference
The Methods Innovation Rule, which
was finalized on June 14, 2005, revised
40 CFR 260.11 to remove the
incorporation by reference of all SW–
846 methods except those SW–846
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00023 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12550
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
13
It is important to note that while a method
listed in §260.11 is a method-defined parameter,
that method also may be used for non-mandatory
purposes. For example, the Pensky-Martens method
described in Method 1010A could also be used as
part of quality control to test a product for purity,
which is unrelated to §261.21 and, otherwise, not
required under RCRA. In this case, the method
would not be a method-defined parameter. In order
to be a method-defined parameter, a method must
be part of a regulatory requirement under RCRA.
14
EPA notes that decisions regarding whether a
state rule is more stringent or broader in scope than
the federal program are made when the Agency
authorizes a state program for a particular rule.
methods that are also regulatory
required method-defined parameters.
Those methods remain incorporated by
reference when used as method-defined
parameters under the RCRA regulations
and, thus, can only be amended through
a regulatory effort.
13
The Agency is proposing to
incorporate by reference ASTM D 8174–
18, ASTM D 8175–18, ASTM E 681–85,
SW–846 Method 1010B and SW–846
Method 1020C into § 261.21 and as
applicable into Appendix IX to part 261.
These test methods are described in
detail in Section III and Section V,
above. The Agency is also proposing to
incorporate by reference SW–846 Test
Methods 0010, 0011, 0020, 0023A, and
0051. These test methods are updated
versions of currently incorporated by
reference SW–846 Methods 0010, 0011,
0020, 0023A, and 0051, as described in
Section VI, above. The Agency is
proposing to incorporate by reference
Method 0010 into § 260.11(c)(3)(i) and
Appendix IX to part 261. The Agency is
proposing to incorporate by reference
Method 0011 into § 260.11(c)(3)(viii)
and Appendix IX to part 261. The
Agency is proposing to incorporate by
reference Method 0020 into
§ 260.11(c)(3)(ii) and Appendix IX to
part 261. The Agency is proposing to
incorporate by reference Method 0023A
into§ 260.11(c)(3)(ix) Appendix IX to
part 261, § 266.104(e)(1), and Appendix
IX to part 266. The Agency is proposing
to incorporate by reference Method 0051
into § 260.11(c)(3)(xiii), Appendix IX to
part 261, § 266.107(f), and Appendix IX
to part 266. The Agency is also
proposing to incorporate by reference
Method 0011 into § 260.11(c)(3)(viii)
and Appendix IX to part 266. The
ASTM standards proposed for
incorporation by reference are available
for purchase from ASTM International,
100 Barr Harbor Drive, P.O. Box C700,
West Conshohocken, PA 19428–2959,
www.astm.org, 877–909–2786. To obtain
ASTM E 681–85, call 877–909–2786.
The SW–846 Test Methods proposed for
incorporation by reference are
published in the test methods
compendium known as ‘‘Test Methods
for Evaluating Solid Waste, Physical/
Chemical Methods,’’ EPA Publication
SW–846, Third Edition, available at
https://www.epa.gov/hw-sw846.
VIII. State Authorization
A. Applicability of Proposed Rule in
Authorized States
Under section 3006 of RCRA, EPA
may authorize qualified states to
administer and enforce the RCRA
hazardous waste program within the
state. Following authorization, EPA
retains enforcement authority under
sections 3008, 3013, and 7003 of RCRA,
although authorized states have primary
enforcement responsibility. The
standards and requirements for state
authorization are found at 40 CFR part
271. Prior to enactment of the
Hazardous and Solid Waste
Amendments of 1984 (HSWA), a state
with final RCRA authorization
administered its hazardous waste
program entirely in lieu of EPA
administering the federal program in
that state. The federal requirements no
longer applied in the authorized state,
and EPA could not issue permits for any
facilities in that state, since only the
state was authorized to issue RCRA
permits. When EPA promulgated new,
more stringent federal requirements for
these pre-HSWA regulations, the state
was obligated to enact equivalent
authorities within specified time frames.
However, the new federal requirements
did not take effect in an authorized
state, until the state adopted the federal
requirements as state law. In contrast,
under RCRA section 3006(g) (42 U.S.C.
6926(g)), which was added by HSWA,
new requirements and prohibitions
imposed under HSWA authority take
effect in authorized states at the same
time that they take effect in
unauthorized states. EPA is directed by
the statute to implement these
requirements and prohibitions in
authorized states, including the
issuance of permits, until the state is
granted authorization to do so. While
states must still adopt HSWA related
provisions as state law to retain final
authorization, EPA implements the
HSWA provisions in authorized states
until the states do so.
Authorized states are required to
modify their programs only when EPA
enacts federal requirements that are
more stringent or broader in scope than
existing federal requirements.
14
RCRA
section 3009 allows the states to impose
standards more stringent than those in
the federal program (see also 40 CFR
271.1). Therefore, authorized states may,
but are not required to, adopt federal
regulations, both HSWA and non-
HSWA, that are considered less
stringent than previous federal
regulations.
B. Effect on State Authorization
Today’s notice proposes regulations
that, if finalized, would not be
promulgated under the authority of
HSWA. Thus, the standards, if finalized,
would be applicable on the effective
date only in those states that do not
have final authorization of their base
RCRA programs. Moreover, authorized
states are required to modify their
programs only when EPA promulgates
federal regulations that are more
stringent or broader in scope than the
authorized state regulations. For those
changes that are less stringent, states are
not required to modify their programs.
This is a result of section 3009 of RCRA,
which allows states to impose more
stringent regulations than the federal
program.
The proposed revisions to several test
methods are considered to be neither
more nor less stringent than the existing
test methods. Thus, authorized states
may, but are not required to, adopt these
changes.
IX. Statutory and Executive Orders
Reviews
Additional information about these
statutes and Executive Orders can be
found at http://www.epa.gov/laws-
regulations/laws-and-executive-orders.
A. Executive Order 12866: Regulatory
Planning and Review and Executive
Order 13563: Improving Regulation and
Regulatory Review
This action is not a significant
regulatory action because it does not
have a significant economic impact nor
does it raise novel legal or policy issues.
The Office of Management and Budget
(OMB) waived review.
B. Executive Order 13771: Reducing
Regulations and Controlling Regulatory
Costs
This action is expected to be an
Executive Order 13771 deregulatory
action. Details on the estimated cost
savings of this proposed rule can be
found in EPA’s Regulatory Impact
Analysis of the Modernization of
Ignitable Liquid Determination Rule,
which is in the docket.
C. Paperwork Reduction Act (PRA)
The use of the proposed methods or
the existing methods impose the same
information collection burden as the
existing regulation. OMB has previously
approved the information collection
activities contained in the existing
regulations and has assigned OMB
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00024 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12551
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
control numbers 2050–0053 and 2050–
0073.
D. Regulatory Flexibility Act (RFA)
I certify that this proposed action will
not have a significant economic impact
on a substantial number of small entities
under the RFA. In making this
determination, the impact of concern is
any significant adverse economic
impact on small entities. An agency may
certify that a rule will not have a
significant economic impact on a
substantial number of small entities if
the rule relieves regulatory burden, has
no net burden or otherwise has a
positive economic effect on the small
entities subject to the rule. As
documented in the Regulatory Impact
Analysis of the Modernization of
Ignitable Liquid Determinations Rule
found in the docket for this proposal,
EPA does not expect the rule to result
in an adverse impact to a significant
number of small entities. For
commercial labs, the analysis presented
in Chapter 3 indicates either no change
in costs or a cost savings, due to the
flexibility afforded by the rule.
Therefore, out of the 128 firms defined
as small under the Small Business
Administration size standards, no firms
have costs greater than one percent of
annual revenues. EPA has therefore
concluded that this proposed action will
either relieve regulatory burden or have
no net regulatory burden for all directly
regulated small entities.
E. Unfunded Mandates Reform Act
(UMRA)
As documented in the Regulatory
Impact Analysis of the Modernization of
Ignitable Liquid Determinations Rule
found in the docket for this proposal,
this proposed action does not contain an
unfunded mandate of $100 million or
more as described in UMRA, 2 U.S.C.
1531–1538, and does not significantly or
uniquely affect small governments.
F. Executive Order 13132: Federalism
This action does not have federalism
implications. It will not have substantial
direct effects on the states, on the
relationship between the national
government and the states, or on the
distribution of power and
responsibilities among the various
levels of government.
G. Executive Order 13175: Consultation
and Coordination With Indian Tribal
Governments
This proposed action does not have
tribal implications as specified in
Executive Order 13175. Because the
proposed rule is expected to result in
minimal costs and possibly net cost
savings, EPA does not expect that it
would result in any adverse impacts on
tribal entities. Thus, Executive Order
13175 does not apply to this rule.
H. Executive Order 13045: Protection of
Children From Environmental Health
Risks and Safety Risks
The EPA interprets Executive Order
13045 as applying only to those
regulatory actions that concern
environmental health or safety risks that
the EPA has reason to believe may
disproportionately affect children, per
the definition of ‘‘covered regulatory
action’’ in section 2–202 of the
Executive Order. This action is not
subject to Executive Order 13045
because it does not concern an
environmental health risk or safety risk.
I. Executive Order 13211: Actions
Concerning Regulations That
Significantly Affect Energy Supply,
Distribution or Use
This action is not subject to Executive
Order 13211, because it is not a
significant regulatory action under
Executive Order 12866.
J. National Technology Transfer and
Advancement Act (NTTAA)
This action involves technical
standards. The EPA proposes to use
ASTM D 8175–18 and ASTM D 8174–
18. These test methods were adopted by
ASTM in March 2018. These standards
are available for purchase from ASTM
International, 100 Barr Harbor Drive,
P.O. Box C700, West Conshohocken, PA
19428–2959. EPA worked with ASTM to
specifically develop these consensus-
based standards to better suit waste
testing by modifying existing ASTM
standards. EPA worked with a member
of the ASTM D02.08 Subcommittee
(who also represents Stanhope-Seta) to
modify existing ASTM methods D 93–
16 and D 3828–16a, which were
developed by the ASTM D02.08
Subcommittee. These new draft
methods were then submitted to
ASTM’s review process and were
approved by the ASTM D34 Committee
to become new ASTM methods.
K. Executive Order 12898: Federal
Actions To Address Environmental
Justice in Minority Populations and
Low-Income Populations
The EPA believes that this action does
not have disproportionately high and
adverse human health or environmental
effects on minority populations, low-
income populations and/or indigenous
peoples, as specified in Executive Order
12898 (59 FR 7629, February 16, 1994).
This proposed rule would only
modernize testing and codify guidance
for the characterization of ignitable
hazardous waste, it would not affect
how such waste is disposed of. EPA
therefore does not expect it to result in
any adverse environmental justice
impacts.
List of Subjects
40 CFR Part 260
Environmental protection,
Administrative practice and procedure,
Confidential business information,
Hazardous waste, Incorporation by
reference, Reporting and recordkeeping
requirements.
40 CFR Part 261
Environmental protection, Hazardous
waste, Incorporation by reference,
Recycling, Reporting and recordkeeping
requirements.
40 CFR Part 266
Environmental protection, Energy,
Hazardous waste, Incorporation by
reference, Recycling, Reporting and
recordkeeping requirements.
Dated: March 21, 2019.
Andrew R. Wheeler,
Administrator.
For the reasons set forth in the
preamble, EPA proposes to amend 40
CFR parts 260 and 261 as follows:
PART 260—HAZARDOUS WASTE
MANAGEMENT SYSTEM: GENERAL
1. The authority citation for part 260
continues to read as follows:
Authority: 42 U.S.C. 6905, 6912(a), 6921–
6927, 6930, 6934, 6935, 6937, 6938, 6939,
and 6974.
2. Amend § 260.11 by:
a. Adding new paragraphs (b)(11)
through (13); and
b. Revising paragraphs (c)(3)(i), (ii),
(viii), (ix), (xiii), (xvii), and (xviii).
The additions and revisions read as
follows:
§ 260.11 Incorporation by reference.
* * * * *
(b) * * *
* * * * *
(11) ASTM D 8175–18 ‘‘Test Method
for Finite Flash Point Determination of
Liquid Wastes by Pensky-Martens
Closed Cup Tester.’’ IBR approved for
§ 261.21.
(12) ASTM D 8174–18 ‘‘Test Method
for Finite Flash Point Determination of
Liquid Wastes by Small Scale Closed
Cup Tester.’’ IBR approved for § 261.21.
(13) ASTM E 681–85 ‘‘Standard Test
Method for Concentration Limits of
Flammability of Chemicals (Vapors and
gases).’’ IBR approved for § 261.21.
(c) * * *
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00025 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS
12552
Federal Register / Vol. 84, No. 63 / Tuesday, April 2, 2019 / Proposed Rules
(3) * * *
(i) Method 0010, dated [TBD] and in
the Basic Manual, IBR approved for
appendix IX to part 261.
(ii) Method 0020, dated [TBD] and in
the Basic Manual, IBR approved for
appendix IX to part 261.
* * * * *
(viii) Method 0011, dated [TBD] and
in Update III, IBR approved for
appendix IX to part 261 and appendix
IX to part 266,.
(ix) Method 0023A, dated [TBD] and
in Update III, IBR approved for
appendix IX to part 261, § 266.104, and
appendix IX to part 266, ,.
* * * * *
(xiii) Method 0051, dated [TBD] and
in Update III, IBR approved for
appendix IX to part 261, § 266.107, and
appendix IX to part 266,
* * * * *
(xvii) Method 1010B, dated December
2018 and in Update VII, IBR approved
for § 261.21 and appendix IX to part
261.
(xviii) Method 1020C, dated
December 2018 and in Update VII, IBR
approved for § 261.21 and appendix IX
to part 261.
* * * * *
PART 261—IDENTIFICATION AND
LISTING OF HAZARDOUS WASTE
3.The authority citation for part 261
continues to read as follows:
Authority: 42 U.S.C. 6905, 6912(a), 6921,
6922, 6924(y) and 6938.
4. Amend § 261.21 by:
a. Revising paragraphs (a)(1), (3)(ii),
and (4)(i)(A) adding paragraph (a)(5);
and
b. Removing Notes 1, 2, 3, and 4 to
read as follows:
§ 261.21 Characteristic of ignitability.
(a) * * *
(1) It is a liquid, other than a solution
containing less than 24 percent of any
alcohol or combination of alcohols
(except if the alcohol has been used for
its solvent properties and is one of the
alcohols specified in EPA Hazardous
Waste No. F003 or F005 in 40 CFR
261.31) by volume and at least 50
percent water by weight, that has a flash
point less than 60 °C (140 °F), as
determined by using one of the
following ASTM standards: ASTM D
93–79, D 93–80, D 3278–78, D 8174–18
or D 8175–18 as specified in SW–846
Test Methods 1010B or 1020C
(incorporated by reference, see § 260.11
of this subchapter).
* * * * *
(3) * * *
(ii) A compressed gas shall be
characterized as ignitable if any one of
the following occurs:
(A) Either a mixture of 13 percent or
less (by volume) with air forms a
flammable mixture or the flammable
range with air is wider than 12 percent
regardless of the lower limit. These
limits shall be determined at
atmospheric temperature and pressure.
The method of sampling and test
procedure shall be the ASTM E 681–85
(incorporated by reference, see § 260.11
of this subchapter), or other equivalent
methods approved by the Associate
Administrator, Pipeline and Hazardous
Materials Safety Administration, U.S.
Department of Transportation.
(B) It is determined to be flammable
or extremely flammable using 49 CFR
173.115(l).
(4) * * *
(i) * * *
(A) The material meets the definition
of a Division1.1, 1.2, or 1.3 explosive, as
defined in § 261.23(a)(8), in which case
it must be classed as an explosive,
* * * * *
(5) It is a multiphase mixture, where
any liquid phase has the flash point
described in paragraph (a)(1) of this
section, or any non-liquid phase has the
properties described in paragraph (a)(2)
of this section.
* * * * *
5. Amend Tables 1 and 2 of Appendix
IX to Part 261 by removing the text
‘‘1010A’’ and adding ‘‘1010B’’ in its
place, wherever it appears (56
occurrences); and removing the text
‘‘1020B’’ and adding ‘‘1020C’’ in its
place, wherever it appears (56
occurrences).
[FR Doc. 2019–05878 Filed 4–1–19; 8:45 am]
BILLING CODE 6560–50–P
DEPARTMENT OF HEALTH AND
HUMAN SERVICES
Centers for Medicare & Medicaid
Services
42 CFR Part 600
[CMS–2407–PN]
RIN 0938–ZB42
Basic Health Program; Federal
Funding Methodology for Program
Years 2019 and 2020
AGENCY
: Centers for Medicare &
Medicaid Services (CMS), HHS.
ACTION
: Proposed methodology.
SUMMARY
: This document proposes the
methodology and data sources necessary
to determine federal payment amounts
to be made in program years 2019 and
2020 to states that elect to establish a
Basic Health Program under the Patient
Protection and Affordable Care Act to
offer health benefits coverage to low-
income individuals otherwise eligible to
purchase coverage through Affordable
Insurance Exchanges. Prior to the final
notice being published, Basic Health
Program (BHP) payments will be made
using the methodology described in the
Final Administrative Order published
on August 24, 2018. Payments for 2019
will be conformed to the finalized 2019
payment methodology through
reconciliation.
DATES
: To be assured consideration,
comments must be received at one of
the addresses provided below, no later
than 5 p.m. on May 2, 2019.
ADDRESSES
: In commenting, refer to file
code CMS–2407–PN. Because of staff
and resource limitations, we cannot
accept comments by facsimile (FAX)
transmission.
Comments, including mass comment
submissions, must be submitted in one
of the following three ways (please
choose only one of the ways listed):
1. Electronically. You may submit
electronic comments on this regulation
to http://www.regulations.gov. Follow
the ‘‘Submit a comment’’ instructions.
2. By regular mail. You may mail
written comments to the following
address ONLY: Centers for Medicare &
Medicaid Services, Department of
Health and Human Services, Attention:
CMS–2407–PN, P.O. Box 8016,
Baltimore, MD 21244–8016.
Please allow sufficient time for mailed
comments to be received before the
close of the comment period.
3. By express or overnight mail. You
may send written comments to the
following address ONLY: Centers for
Medicare & Medicaid Services,
Department of Health and Human
Services, Attention: CMS–2407–PN,
Mail Stop C4–26–05, 7500 Security
Boulevard, Baltimore, MD 21244–1850.
For information on viewing public
comments, see the beginning of the
SUPPLEMENTARY INFORMATION
section.
FOR FURTHER INFORMATION CONTACT
:
Christopher Truffer, (410) 786–1264; or
Cassandra Lagorio, (410) 786–4554.
SUPPLEMENTARY INFORMATION
:
Inspection of Public Comments: All
comments received before the close of
the comment period are available for
viewing by the public, including any
personally identifiable or confidential
business information that is included in
a comment. We post all comments
received before the close of the
VerDate Sep<11>2014 17:52 Apr 01, 2019 Jkt 247001 PO 00000 Frm 00026 Fmt 4702 Sfmt 4702 E:\FR\FM\02APP1.SGM 02APP1
amozie on DSK9F9SC42PROD with PROPOSALS

VLEX uses login cookies to provide you with a better browsing experience. If you click on 'Accept' or continue browsing this site we consider that you accept our cookie policy. ACCEPT